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14N NMR Spectrum

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Axel Schulz – One of the best experts on this subject based on the ideXlab platform.

  • Characterization, Crystal Structure of 2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a]-[1,3,5]triazine, and Improved Crystal Structure of 2,4,6-Triazido-1,3,5-triazine
    European Journal of Inorganic Chemistry, 1998
    Co-Authors: Elmar Keßenich, Thomas M. Klapötke, Jörg Knizek, Heinrich Nöth, Axel Schulz

    Abstract:

    2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a][1,3,5]triazine (1) was synthesized by reaction of cyanuric azide with triphenylphosphane. 1 is characterized by X-ray structural analysis, IR, Raman, and NMR spectroscopy. The obtained spectra showed that the remaining azide group in 1 reacts with the N4 atom of the triazine ring and forms a tetrazole. An improved crystal structure for 2,4,6-triazido-1,3,5-triazine (2) was determined and for the first time a 14NNMR Spectrum was obtained. CAUTION: 2 (Cyanuric azide) is explosive! The explosive nature increases with greater purity and crystal size.

Elmar Keßenich – One of the best experts on this subject based on the ideXlab platform.

  • Characterization, Crystal Structure of 2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a]-[1,3,5]triazine, and Improved Crystal Structure of 2,4,6-Triazido-1,3,5-triazine
    European Journal of Inorganic Chemistry, 1998
    Co-Authors: Elmar Keßenich, Thomas M. Klapötke, Jörg Knizek, Heinrich Nöth, Axel Schulz

    Abstract:

    2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a][1,3,5]triazine (1) was synthesized by reaction of cyanuric azide with triphenylphosphane. 1 is characterized by X-ray structural analysis, IR, Raman, and NMR spectroscopy. The obtained spectra showed that the remaining azide group in 1 reacts with the N4 atom of the triazine ring and forms a tetrazole. An improved crystal structure for 2,4,6-triazido-1,3,5-triazine (2) was determined and for the first time a 14NNMR Spectrum was obtained. CAUTION: 2 (Cyanuric azide) is explosive! The explosive nature increases with greater purity and crystal size.

Jörg Knizek – One of the best experts on this subject based on the ideXlab platform.

  • Characterization, Crystal Structure of 2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a]-[1,3,5]triazine, and Improved Crystal Structure of 2,4,6-Triazido-1,3,5-triazine
    European Journal of Inorganic Chemistry, 1998
    Co-Authors: Elmar Keßenich, Thomas M. Klapötke, Jörg Knizek, Heinrich Nöth, Axel Schulz

    Abstract:

    2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a][1,3,5]triazine (1) was synthesized by reaction of cyanuric azide with triphenylphosphane. 1 is characterized by X-ray structural analysis, IR, Raman, and NMR spectroscopy. The obtained spectra showed that the remaining azide group in 1 reacts with the N4 atom of the triazine ring and forms a tetrazole. An improved crystal structure for 2,4,6-triazido-1,3,5-triazine (2) was determined and for the first time a 14NNMR Spectrum was obtained. CAUTION: 2 (Cyanuric azide) is explosive! The explosive nature increases with greater purity and crystal size.