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14N NMR Spectrum
The Experts below are selected from a list of 8772 Experts worldwide ranked by ideXlab platform
Axel Schulz – One of the best experts on this subject based on the ideXlab platform.
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Characterization, Crystal Structure of 2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a]-[1,3,5]triazine, and Improved Crystal Structure of 2,4,6-Triazido-1,3,5-triazine
European Journal of Inorganic Chemistry, 1998Co-Authors: Elmar Keßenich, Thomas M. Klapötke, Jörg Knizek, Heinrich Nöth, Axel SchulzAbstract:2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a][1,3,5]triazine (1) was synthesized by reaction of cyanuric azide with triphenylphosphane. 1 is characterized by X-ray structural analysis, IR, Raman, and NMR spectroscopy. The obtained spectra showed that the remaining azide group in 1 reacts with the N4 atom of the triazine ring and forms a tetrazole. An improved crystal structure for 2,4,6-triazido-1,3,5-triazine (2) was determined and for the first time a 14N–NMR Spectrum was obtained. CAUTION: 2 (Cyanuric azide) is explosive! The explosive nature increases with greater purity and crystal size.
Elmar Keßenich – One of the best experts on this subject based on the ideXlab platform.
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Characterization, Crystal Structure of 2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a]-[1,3,5]triazine, and Improved Crystal Structure of 2,4,6-Triazido-1,3,5-triazine
European Journal of Inorganic Chemistry, 1998Co-Authors: Elmar Keßenich, Thomas M. Klapötke, Jörg Knizek, Heinrich Nöth, Axel SchulzAbstract:2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a][1,3,5]triazine (1) was synthesized by reaction of cyanuric azide with triphenylphosphane. 1 is characterized by X-ray structural analysis, IR, Raman, and NMR spectroscopy. The obtained spectra showed that the remaining azide group in 1 reacts with the N4 atom of the triazine ring and forms a tetrazole. An improved crystal structure for 2,4,6-triazido-1,3,5-triazine (2) was determined and for the first time a 14N–NMR Spectrum was obtained. CAUTION: 2 (Cyanuric azide) is explosive! The explosive nature increases with greater purity and crystal size.
Jörg Knizek – One of the best experts on this subject based on the ideXlab platform.
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Characterization, Crystal Structure of 2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a]-[1,3,5]triazine, and Improved Crystal Structure of 2,4,6-Triazido-1,3,5-triazine
European Journal of Inorganic Chemistry, 1998Co-Authors: Elmar Keßenich, Thomas M. Klapötke, Jörg Knizek, Heinrich Nöth, Axel SchulzAbstract:2,4-Bis(triphenylphosphanimino)tetrazolo[5,1-a][1,3,5]triazine (1) was synthesized by reaction of cyanuric azide with triphenylphosphane. 1 is characterized by X-ray structural analysis, IR, Raman, and NMR spectroscopy. The obtained spectra showed that the remaining azide group in 1 reacts with the N4 atom of the triazine ring and forms a tetrazole. An improved crystal structure for 2,4,6-triazido-1,3,5-triazine (2) was determined and for the first time a 14N–NMR Spectrum was obtained. CAUTION: 2 (Cyanuric azide) is explosive! The explosive nature increases with greater purity and crystal size.