Coupled Device

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Alan H. Windle - One of the best experts on this subject based on the ideXlab platform.

  • A novel polymer fibre diffractometer based on a scanning x-ray sensitive charge-Coupled Device
    Journal of Applied Crystallography, 1995
    Co-Authors: Simon Hanna, Alan H. Windle
    Abstract:

    This paper describes the development of a novel X-ray diffractometer, designed for the study of highly uniaxially oriented polymer fibres. The system is designed around a commercial X-ray-sensitive video camera, which is mounted on a three-circle goniometer. The active element in the X-ray camera is a charge-Coupled Device (CCD). The data-collection procedure consists of the combination of several diffraction images, obtained with the detector centred at different points in reciprocal space, to construct a composite diffraction pattern representing a linearized section through the symmetry axis of cylindrically averaged reciprocal space. By the combination of several images in this way, it is possible to overcome the traditional problem in fibre photography of information loss, caused by the Ewald-sphere curvature, close to the reciprocal fibre axis. Methods for optimizing the performance of the CCD detector, in terms of both its resolution and sensitivity, are discussed, and the data gathering and processing system is described in some detail. The operation of the system is demonstrated using samples of liquid-crystalline and conventional synthetic polymeric fibres.

Simon Hanna - One of the best experts on this subject based on the ideXlab platform.

  • A novel polymer fibre diffractometer based on a scanning x-ray sensitive charge-Coupled Device
    Journal of Applied Crystallography, 1995
    Co-Authors: Simon Hanna, Alan H. Windle
    Abstract:

    This paper describes the development of a novel X-ray diffractometer, designed for the study of highly uniaxially oriented polymer fibres. The system is designed around a commercial X-ray-sensitive video camera, which is mounted on a three-circle goniometer. The active element in the X-ray camera is a charge-Coupled Device (CCD). The data-collection procedure consists of the combination of several diffraction images, obtained with the detector centred at different points in reciprocal space, to construct a composite diffraction pattern representing a linearized section through the symmetry axis of cylindrically averaged reciprocal space. By the combination of several images in this way, it is possible to overcome the traditional problem in fibre photography of information loss, caused by the Ewald-sphere curvature, close to the reciprocal fibre axis. Methods for optimizing the performance of the CCD detector, in terms of both its resolution and sensitivity, are discussed, and the data gathering and processing system is described in some detail. The operation of the system is demonstrated using samples of liquid-crystalline and conventional synthetic polymeric fibres.

Richard H. Scheller - One of the best experts on this subject based on the ideXlab platform.

  • Fluorescence detection in capillary zone electrophoresis using a charge-Coupled Device with time-delayed integration.
    Analytical chemistry, 1991
    Co-Authors: Jonathan V. Sweedler, Jason B. Shear, Harvey A. Fishman, Richard N. Zare, Richard H. Scheller
    Abstract:

    A fluorescence detection system for capillary zone electrophoresis is described in which a charged-Coupled Device (CCD) views a 2-cm section of an axially illuminated capillary column. The CCD is operated in two readout modes: a snapshot mode that acquires a series of images in wavelength and capillary position, and a time-delayed integration mode that allows long exposure times of the moving analyte zones. By use of the latter mode, the ability to differentiate a species based on both its fluorescence emission and migration rate is demonstrated for fluorescein and sulforhodamine 101. The detection limit for fluorescein isothiocyanate (FITC) is 1.2 X 10(-20) mol; detection limits for FITC-amino acids are in the (2-8) X 10(-20) mol range.

Peter Kohl - One of the best experts on this subject based on the ideXlab platform.

Eric Lantz - One of the best experts on this subject based on the ideXlab platform.