The Experts below are selected from a list of 246 Experts worldwide ranked by ideXlab platform
Qing Lin - One of the best experts on this subject based on the ideXlab platform.
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Synthesis of Azobenzenes Using N-Chlorosuccinimide and 1,8-Diazabicyclo[5.4.0]undec-7-ene (DBU)
The Journal of organic chemistry, 2017Co-Authors: Alford A. John, Qing LinAbstract:A convenient method for the synthesis of symmetrical azobenzenes is reported. This one-step procedure involves treatment of anilines with N-Chlorosuccinimide (NCS) and organic base 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU). A wide range of commercially available substituted anilines readily participate in this reaction to produce the corresponding azobenzenes in moderate-to-excellent yields in minutes.
P F Misco - One of the best experts on this subject based on the ideXlab platform.
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oxidation of alcohols by methyl sulfide n chlorosuccinimide triethylamine 4 tert butylcyclohexanone
Organic Syntheses, 2003Co-Authors: E J Corey, C U Kim, P F MiscoAbstract:Oxidation of alcohols by methyl sulfide- N-Chlorosuccinimide- triethylamine: 4-tert-butylcyclohexanone catalyst: 8.0 g. (0.060 mole) of N-Chlorosuccinimide product: 4-tert-butylcyclohexanone byproduct: 4-tert-butylcyclohexylmethyl methylthiomethyl ether product: C6H5CHO Keywords: oxidation, CHOH CO; N-Chlorosuccinimide; dimethyl sulfoxide-methyl sulfide reagent
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Organic Syntheses - Oxidation of Alcohols by Methyl Sulfide‐ N‐Chlorosuccinimide‐ Triethylamine: 4‐tert‐Butylcyclohexanone
Organic Syntheses, 2003Co-Authors: E J Corey, C U Kim, P F MiscoAbstract:Oxidation of alcohols by methyl sulfide- N-Chlorosuccinimide- triethylamine: 4-tert-butylcyclohexanone catalyst: 8.0 g. (0.060 mole) of N-Chlorosuccinimide product: 4-tert-butylcyclohexanone byproduct: 4-tert-butylcyclohexylmethyl methylthiomethyl ether product: C6H5CHO Keywords: oxidation, CHOH CO; N-Chlorosuccinimide; dimethyl sulfoxide-methyl sulfide reagent
Alford A. John - One of the best experts on this subject based on the ideXlab platform.
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Synthesis of Azobenzenes Using N-Chlorosuccinimide and 1,8-Diazabicyclo[5.4.0]undec-7-ene (DBU)
The Journal of organic chemistry, 2017Co-Authors: Alford A. John, Qing LinAbstract:A convenient method for the synthesis of symmetrical azobenzenes is reported. This one-step procedure involves treatment of anilines with N-Chlorosuccinimide (NCS) and organic base 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU). A wide range of commercially available substituted anilines readily participate in this reaction to produce the corresponding azobenzenes in moderate-to-excellent yields in minutes.
E J Corey - One of the best experts on this subject based on the ideXlab platform.
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oxidation of alcohols by methyl sulfide n chlorosuccinimide triethylamine 4 tert butylcyclohexanone
Organic Syntheses, 2003Co-Authors: E J Corey, C U Kim, P F MiscoAbstract:Oxidation of alcohols by methyl sulfide- N-Chlorosuccinimide- triethylamine: 4-tert-butylcyclohexanone catalyst: 8.0 g. (0.060 mole) of N-Chlorosuccinimide product: 4-tert-butylcyclohexanone byproduct: 4-tert-butylcyclohexylmethyl methylthiomethyl ether product: C6H5CHO Keywords: oxidation, CHOH CO; N-Chlorosuccinimide; dimethyl sulfoxide-methyl sulfide reagent
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Organic Syntheses - Oxidation of Alcohols by Methyl Sulfide‐ N‐Chlorosuccinimide‐ Triethylamine: 4‐tert‐Butylcyclohexanone
Organic Syntheses, 2003Co-Authors: E J Corey, C U Kim, P F MiscoAbstract:Oxidation of alcohols by methyl sulfide- N-Chlorosuccinimide- triethylamine: 4-tert-butylcyclohexanone catalyst: 8.0 g. (0.060 mole) of N-Chlorosuccinimide product: 4-tert-butylcyclohexanone byproduct: 4-tert-butylcyclohexylmethyl methylthiomethyl ether product: C6H5CHO Keywords: oxidation, CHOH CO; N-Chlorosuccinimide; dimethyl sulfoxide-methyl sulfide reagent
Yasuhiko Kurusu - One of the best experts on this subject based on the ideXlab platform.
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Imine allylations by Allylic trichlorotins derived from α, α-diisopropylhomo-allylic alcohols with tin(II) chloride and N-Chlorosuccinimide
Synlett, 2002Co-Authors: Yoshiro Masuyama, Naoko Yamamoto, Yasuhiko KurusuAbstract:Allylic trichlorotins, prepared in situ from α,α-diisopropylhomoallylic alcohols with tin(II) chloride and N-Chlorosuccinimide in dichloromethane at -40 °C, cause nucleophilic addition to N-tosylimines or N-tosyliminiums to afford the corresponding α-substituted homoallylic amines.
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Imine allylation by allylic trimethylsilanes via in situ formation of N-tosyliminium species from carbonyl compounds and toluene-p-sulfonamide with SnCl2 and N-Chlorosuccinimide: regioselection and diastereoselection
Chemical Communications, 1999Co-Authors: Yoshiro Masuyama, Jiro Tosa, Yasuhiko KurusuAbstract:N-Tosyliminium species, prepared in situ from carbonyl compounds and TsNH2 with SnCl2 and N-Chlorosuccinimide, undergo nucleophilic addition of allylic silanes (imine allylation) to produce the corresponding homoallylic amines; the imine allylation by but-2-enyltrimethylsilane with aldehydes and TsNH2 leads to regio- and diastereo-selection to produce anti 1-substituted 2-methylbut-3-enylamines.
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Ring Construction of Homoallylic Alcohols and Aldehydes with N-Chlorosuccinimide/Tin(II) Chloride
Synthetic Communications, 1995Co-Authors: Yoshiro Masuyama, Shin-yah Gotoh, Yasuhiko KurusuAbstract:Abstract The reaction of homoallylic alcohols and aldehydes with N-Chlorosuccinimide/tin(II) chloride in dichloromethane led to ring construction to produce 2-substituted 4-chlorotetrahydropyrans diastereoselectively.
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Aldol reaction of enol acetates and lactols with N-Chlorosuccinimide and tin(II) chloride. Diastereoselective synthesis of disubstituted cyclic ethers
Journal of the Chemical Society Chemical Communications, 1994Co-Authors: Yoshiro Masuyama, Yumiko Kobayashi, Yasuhiko KurusuAbstract:Lactols reacted with enol acetates by a Lewis acid reagent, derived from N-Chlorosuccinimide and tin(II) chloride, to produce 2-acetonyl cyclic ethers diastereoselectively.