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Panagiotis Lianos - One of the best experts on this subject based on the ideXlab platform.

Elias Stathatos - One of the best experts on this subject based on the ideXlab platform.

Tatsuya Sekine - One of the best experts on this subject based on the ideXlab platform.

Bing Yan - One of the best experts on this subject based on the ideXlab platform.

  • lanthanide eu3 tb3 β diketone modified mesoporous sba 15 organic polymer hybrids chemically bonded construction physical characterization and photophysical properties
    Inorganic Chemistry, 2009
    Co-Authors: Bing Yan
    Abstract:

    Novel organic−inorganic mesoporous luminescent polymeric hybrid materials containing lanthanide (Eu3+, Tb3+) complexes covalently bonded to mesoporous silica SBA-15 have been successfully prepared by co-condensation of the modified 2-Thenoyltrifluoroacetone (TTA−Si) and tetraethoxysilane (TEOS) in the presence of Pluronic P123 surfactant as a template. 2Z-Thenoyltrifluoroacetone (TTA) was grafted onto the coupling agent 3-(triethoxysilyl)-propyl isocyanate (TEPIC) and used as the first precursor, and the other precursor PMMA was synthesized through the addition polymerization reaction of the monomer methyl methacrylate. Then these precursors coordinated to rare earth ions, and the final mesoporous polymeric hybrid materials Ln(TTA-SBA-15)3PMMA (Ln = Eu, Tb) were obtained after hydrolysis and copolycondensation with the tetraethoxysilane (TEOS) via a sol−gel process. In addition, for comparison, SBA-15 covalently bonded with the binary Ln3+ complexes with TTA ligand were also synthesized, denoted as Ln(TTA...

  • covalently bonding assembly and photophysical properties of luminescent molecular hybrids eu tta si and eu ttasi mcm 41 by modified Thenoyltrifluoroacetone
    Microporous and Mesoporous Materials, 2009
    Co-Authors: Bing Yan, Bing Zhou
    Abstract:

    Abstract In the context, the two novel kinds of hybrid materials, TTA–Si directly chemically bonded molecular hybrids and the corresponding MCM-41 host assembling hybrids were prepared. The organic–inorganic mesoporous luminescent materials were synthesized by linking Eu 3+ complexes to the functionalized ordered mesoporous MCM-41 with modified Thenoyltrifluoroacetone (TTA–Si) by co-condensation of tetraethoxysilane (TEOS) in the presence of the cetyltrimethylammonium bromide (CTAB) surfactant as template. Thenoyltrifluoroacetone (TTA) was grafted with coupling agent 3-(triethoxysilyl)-propyl isocyanate and the as-derived functional bridge molecule (denoted as TTA–Si) was introduced into inorganic polymeric host MCM-41 through covalent bonds, resulting in the molecular hybrid material. The luminescence properties of these resulting materials were characterized in detail, and the results reveal that they all have high surface area, uniformity in the mesostructure and crystallinity. The efficient intramolecular energy transfer in mesoporous material Eu–TTASi–MCM-41 mainly occurs between the modified ligand TTA–Si and the central Eu 3+ ion. In addition, the constructed covalently bonded hybrids present the longer luminescent lifetimes than common Eu(III) β-diketones complexes for improvement of stability. Especially the mesoporous luminescent material Eu–TTASi–MCM-41possesses high luminescence quantum efficiency .

Kiyoshi Sawada - One of the best experts on this subject based on the ideXlab platform.