The Experts below are selected from a list of 321 Experts worldwide ranked by ideXlab platform
Benjamin Amorelli - One of the best experts on this subject based on the ideXlab platform.
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Organic Syntheses - Thionation: GlcNAc‐Thiazoline Triacetate {(3aR,5R,6S,7R,7aR)‐5‐Acetoxymethyl‐6,7‐Diacetoxy‐2‐Methyl‐5,6,7,7a‐Tetrahydro‐3aH‐Pyrano[3,2‐d]Thiazole}
Organic Syntheses, 2006Co-Authors: Spencer Knapp, Richard A. Huhn, Benjamin AmorelliAbstract:Acetic anhydride N-Acetyl-D-glucosamine 2-Acetamido-2-deoxy-1,3,4,6-tetra-O-acetyl-beta-D-glucopyranose Phosphorus pentasulfide GlcNAc-thiazole triacetate Hexamethyldisiloxane Keywords: Thionation; montmorillonite K-10 clay; sugars. Per-O-acetylation; cyclization; curphey procedure; thiconjugates; glycopeptides; triacetates
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Thionation glcnac thiazoline triacetate 3ar 5r 6s 7r 7ar 5 acetoxymethyl 6 7 diacetoxy 2 methyl 5 6 7 7a tetrahydro 3ah pyrano 3 2 d thiazole
Organic Syntheses, 2006Co-Authors: Spencer Knapp, Richard A. Huhn, Benjamin AmorelliAbstract:Acetic anhydride N-Acetyl-D-glucosamine 2-Acetamido-2-deoxy-1,3,4,6-tetra-O-acetyl-beta-D-glucopyranose Phosphorus pentasulfide GlcNAc-thiazole triacetate Hexamethyldisiloxane Keywords: Thionation; montmorillonite K-10 clay; sugars. Per-O-acetylation; cyclization; curphey procedure; thiconjugates; glycopeptides; triacetates
Rekha Tank - One of the best experts on this subject based on the ideXlab platform.
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Expeditious Microwave-Assisted Thionation with the System PSCl3/H2O/Et3N under Solvent-Free Condition
Journal of Organic Chemistry, 2008Co-Authors: Uma Pathak, Lokesh Kumar Pandey, Rekha TankAbstract:A novel Thionation protocol for carbonyl compounds, with the system PSCl3/H2O/Et3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation.
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expeditious microwave assisted Thionation with the system pscl3 h2o et3n under solvent free condition
Journal of Organic Chemistry, 2008Co-Authors: Uma Pathak, Lokesh Kumar Pandey, Rekha TankAbstract:A novel Thionation protocol for carbonyl compounds, with the system PSCl3/H2O/Et3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation.
Uma Pathak - One of the best experts on this subject based on the ideXlab platform.
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Preparation of Thioflavonesvia Thiophosphoryl Chloride Mediated Cyclodehydrationand Thionation of 1-(2-Hydroxyphenyl)-3-arylpropane-1,3-diones
Synthesis, 2010Co-Authors: Manorama Vimal, Lokesh Kumar Pandey, Uma Pathak, M. V. S. SuryanarayanaAbstract:A simple and convenient one-pot strategy for the prepa ration of thioflavones from 1,3-diketones is described. Cyclodehydration of a range of β-diketones and Thionation of the resulting flavones was achieved using thiophosphoryl chloride (PSCl 3 ) which serves as both a catalyst and thionating agent.
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Expeditious Microwave-Assisted Thionation with the System PSCl3/H2O/Et3N under Solvent-Free Condition
Journal of Organic Chemistry, 2008Co-Authors: Uma Pathak, Lokesh Kumar Pandey, Rekha TankAbstract:A novel Thionation protocol for carbonyl compounds, with the system PSCl3/H2O/Et3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation.
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expeditious microwave assisted Thionation with the system pscl3 h2o et3n under solvent free condition
Journal of Organic Chemistry, 2008Co-Authors: Uma Pathak, Lokesh Kumar Pandey, Rekha TankAbstract:A novel Thionation protocol for carbonyl compounds, with the system PSCl3/H2O/Et3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation.
Spencer Knapp - One of the best experts on this subject based on the ideXlab platform.
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Organic Syntheses - Thionation: GlcNAc‐Thiazoline Triacetate {(3aR,5R,6S,7R,7aR)‐5‐Acetoxymethyl‐6,7‐Diacetoxy‐2‐Methyl‐5,6,7,7a‐Tetrahydro‐3aH‐Pyrano[3,2‐d]Thiazole}
Organic Syntheses, 2006Co-Authors: Spencer Knapp, Richard A. Huhn, Benjamin AmorelliAbstract:Acetic anhydride N-Acetyl-D-glucosamine 2-Acetamido-2-deoxy-1,3,4,6-tetra-O-acetyl-beta-D-glucopyranose Phosphorus pentasulfide GlcNAc-thiazole triacetate Hexamethyldisiloxane Keywords: Thionation; montmorillonite K-10 clay; sugars. Per-O-acetylation; cyclization; curphey procedure; thiconjugates; glycopeptides; triacetates
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Thionation glcnac thiazoline triacetate 3ar 5r 6s 7r 7ar 5 acetoxymethyl 6 7 diacetoxy 2 methyl 5 6 7 7a tetrahydro 3ah pyrano 3 2 d thiazole
Organic Syntheses, 2006Co-Authors: Spencer Knapp, Richard A. Huhn, Benjamin AmorelliAbstract:Acetic anhydride N-Acetyl-D-glucosamine 2-Acetamido-2-deoxy-1,3,4,6-tetra-O-acetyl-beta-D-glucopyranose Phosphorus pentasulfide GlcNAc-thiazole triacetate Hexamethyldisiloxane Keywords: Thionation; montmorillonite K-10 clay; sugars. Per-O-acetylation; cyclization; curphey procedure; thiconjugates; glycopeptides; triacetates
Lokesh Kumar Pandey - One of the best experts on this subject based on the ideXlab platform.
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Preparation of Thioflavonesvia Thiophosphoryl Chloride Mediated Cyclodehydrationand Thionation of 1-(2-Hydroxyphenyl)-3-arylpropane-1,3-diones
Synthesis, 2010Co-Authors: Manorama Vimal, Lokesh Kumar Pandey, Uma Pathak, M. V. S. SuryanarayanaAbstract:A simple and convenient one-pot strategy for the prepa ration of thioflavones from 1,3-diketones is described. Cyclodehydration of a range of β-diketones and Thionation of the resulting flavones was achieved using thiophosphoryl chloride (PSCl 3 ) which serves as both a catalyst and thionating agent.
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Expeditious Microwave-Assisted Thionation with the System PSCl3/H2O/Et3N under Solvent-Free Condition
Journal of Organic Chemistry, 2008Co-Authors: Uma Pathak, Lokesh Kumar Pandey, Rekha TankAbstract:A novel Thionation protocol for carbonyl compounds, with the system PSCl3/H2O/Et3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation.
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expeditious microwave assisted Thionation with the system pscl3 h2o et3n under solvent free condition
Journal of Organic Chemistry, 2008Co-Authors: Uma Pathak, Lokesh Kumar Pandey, Rekha TankAbstract:A novel Thionation protocol for carbonyl compounds, with the system PSCl3/H2O/Et3N has been discovered. Clean, rapid, and efficient synthesis of a variety of thiocarbonyl compounds such as thioamides, thiolactams, thioketones, thioxanthones, and thioacridone can be achieved through this simple and convenient method under solventless condition with microwave irradiation.
