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Ismail Warad - One of the best experts on this subject based on the ideXlab platform.
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one step synthesis of nio nanoparticles via solid state thermal decomposition at low temperature of novel aqua 2 9 dimethyl 1 10 phenanthroline nicl2 complex
International Journal of Molecular Sciences, 2013Co-Authors: Assem Barakat, Mousa Alnoaimi, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Ismail WaradAbstract:NiCl2(C14H12N2)(H2O)) complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired
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One step synthesis of NiO nanoparticles via solid-state thermal decomposition at low-temperature of novel aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 complex.
International Journal of Molecular Sciences, 2013Co-Authors: Assem Barakat, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Mousa Al-noaimi, Ismail WaradAbstract:[NiCl2(C14H12N2)(H2O)] complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired complex, subjected to thermal decomposition at low temperature of 400 °C in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM).
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Article One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel Aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 Complex
2013Co-Authors: Assem Barakat, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Mousa Al-noaimi, Ismail WaradAbstract:Abstract: [NiCl2(C14H12N2)(H2O)] complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired OPEN ACCESS Int. J. Mol. Sci. 2013, 14 23942 complex, subjected to thermal decomposition at low temperature of 400 °C in an ope
Assem Barakat - One of the best experts on this subject based on the ideXlab platform.
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one step synthesis of nio nanoparticles via solid state thermal decomposition at low temperature of novel aqua 2 9 dimethyl 1 10 phenanthroline nicl2 complex
International Journal of Molecular Sciences, 2013Co-Authors: Assem Barakat, Mousa Alnoaimi, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Ismail WaradAbstract:NiCl2(C14H12N2)(H2O)) complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired
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One step synthesis of NiO nanoparticles via solid-state thermal decomposition at low-temperature of novel aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 complex.
International Journal of Molecular Sciences, 2013Co-Authors: Assem Barakat, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Mousa Al-noaimi, Ismail WaradAbstract:[NiCl2(C14H12N2)(H2O)] complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired complex, subjected to thermal decomposition at low temperature of 400 °C in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM).
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Article One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel Aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 Complex
2013Co-Authors: Assem Barakat, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Mousa Al-noaimi, Ismail WaradAbstract:Abstract: [NiCl2(C14H12N2)(H2O)] complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired OPEN ACCESS Int. J. Mol. Sci. 2013, 14 23942 complex, subjected to thermal decomposition at low temperature of 400 °C in an ope
Ahmed Boshaala - One of the best experts on this subject based on the ideXlab platform.
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one step synthesis of nio nanoparticles via solid state thermal decomposition at low temperature of novel aqua 2 9 dimethyl 1 10 phenanthroline nicl2 complex
International Journal of Molecular Sciences, 2013Co-Authors: Assem Barakat, Mousa Alnoaimi, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Ismail WaradAbstract:NiCl2(C14H12N2)(H2O)) complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired
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One step synthesis of NiO nanoparticles via solid-state thermal decomposition at low-temperature of novel aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 complex.
International Journal of Molecular Sciences, 2013Co-Authors: Assem Barakat, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Mousa Al-noaimi, Ismail WaradAbstract:[NiCl2(C14H12N2)(H2O)] complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired complex, subjected to thermal decomposition at low temperature of 400 °C in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM).
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Article One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel Aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 Complex
2013Co-Authors: Assem Barakat, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Mousa Al-noaimi, Ismail WaradAbstract:Abstract: [NiCl2(C14H12N2)(H2O)] complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired OPEN ACCESS Int. J. Mol. Sci. 2013, 14 23942 complex, subjected to thermal decomposition at low temperature of 400 °C in an ope
Salim F Haddad - One of the best experts on this subject based on the ideXlab platform.
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one step synthesis of nio nanoparticles via solid state thermal decomposition at low temperature of novel aqua 2 9 dimethyl 1 10 phenanthroline nicl2 complex
International Journal of Molecular Sciences, 2013Co-Authors: Assem Barakat, Mousa Alnoaimi, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Ismail WaradAbstract:NiCl2(C14H12N2)(H2O)) complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired
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One step synthesis of NiO nanoparticles via solid-state thermal decomposition at low-temperature of novel aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 complex.
International Journal of Molecular Sciences, 2013Co-Authors: Assem Barakat, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Mousa Al-noaimi, Ismail WaradAbstract:[NiCl2(C14H12N2)(H2O)] complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired complex, subjected to thermal decomposition at low temperature of 400 °C in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM).
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Article One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel Aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 Complex
2013Co-Authors: Assem Barakat, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Mousa Al-noaimi, Ismail WaradAbstract:Abstract: [NiCl2(C14H12N2)(H2O)] complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired OPEN ACCESS Int. J. Mol. Sci. 2013, 14 23942 complex, subjected to thermal decomposition at low temperature of 400 °C in an ope
Taibi Ben Hadda - One of the best experts on this subject based on the ideXlab platform.
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one step synthesis of nio nanoparticles via solid state thermal decomposition at low temperature of novel aqua 2 9 dimethyl 1 10 phenanthroline nicl2 complex
International Journal of Molecular Sciences, 2013Co-Authors: Assem Barakat, Mousa Alnoaimi, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Ismail WaradAbstract:NiCl2(C14H12N2)(H2O)) complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired
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One step synthesis of NiO nanoparticles via solid-state thermal decomposition at low-temperature of novel aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 complex.
International Journal of Molecular Sciences, 2013Co-Authors: Assem Barakat, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Mousa Al-noaimi, Ismail WaradAbstract:[NiCl2(C14H12N2)(H2O)] complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired complex, subjected to thermal decomposition at low temperature of 400 °C in an open atmosphere, revealed a novel and facile synthesis of pure NiO nanoparticles with uniform spherical particle; the structure of the NiO nanoparticles product was elucidated on the basis of Fourier transform infrared (FT-IR), UV-vis spectroscopy, TG/DTA, XRD, scanning electron microscopy (SEM), energy-dispersive X-ray spectrometry (EDXS) and transmission electron microscopy (TEM).
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Article One Step Synthesis of NiO Nanoparticles via Solid-State Thermal Decomposition at Low-Temperature of Novel Aqua(2,9-dimethyl-1,10-phenanthroline)NiCl2 Complex
2013Co-Authors: Assem Barakat, Mohammed Suleiman, A S Aldwayyan, B Hammouti, Taibi Ben Hadda, Salim F Haddad, Ahmed Boshaala, Mousa Al-noaimi, Ismail WaradAbstract:Abstract: [NiCl2(C14H12N2)(H2O)] complex has been synthesized from Nickel Chloride Hexahydrate (NiCl2·6H2O) and 2,9-dimethyl-1,10-phenanthroline (dmphen) as N,N-bidentate ligand. The synthesized complex was characterized by elemental analysis, infrared (IR) spectroscopy, ultraviolet-visible (UV-vis) spectroscopy and differential thermal/thermogravimetric analysis (TG/DTA). The complex was further confirmed by single crystal X-ray diffraction (XRD) as triclinic with space group P-1. The desired OPEN ACCESS Int. J. Mol. Sci. 2013, 14 23942 complex, subjected to thermal decomposition at low temperature of 400 °C in an ope