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Supriyadi Supriyadi - One of the best experts on this subject based on the ideXlab platform.
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Perbandingan Ekstraksi Oleoresin Biji Pala (Myrictica Fragrans Houtt) Asal Maluku Utara Menggunakan Metode Maserasi dan Gabungan Distilasi – Maserasi
2013Co-Authors: Muhammad Assagaf, Chusnul Hidayat, Pudji Hastuti, Supriyadi SupriyadiAbstract:The purpose of this study was to compare the composition of oleoresin nutmeg (Myristica fragrans Houtt) madedirectly by maceration and combined distillation – maceration. Nutmeg oleoresin yield amounted to 15.17±0.07 (% db)obtained by direct maceration and oleoresin extraction method combined distillation and maceration obtained yield of20.07±0.23 (% db). While the essential oil yield itself from the water-steam distillation of the results obtained at 6.61(% db). Ethanol extract of oleoresin analysis using GCMS method identiÞ ed a total of 39 kinds of compounds withthe composition of major components is methyleugenol (33.40 %), Myristicine (10.90 %), cis-methyl isoeugenol (9.09%), elemicin (8.33 %), and isocoumarin (5.61 %). For nutmeg essential oil contained 31 components of the compound,where the components are located in large numbers was sabinene (34.97 %), !-phellandrene (19.9 %), methyleugenol(7.55 %), Myristicine (5.29 %) and elimicine (3.21 %). As for the essential oil is mixed with the oleoresin from the pulpremaining distillation contained 58 components that make up the compound of the oleoresin with a mixture of maincomponents, namely: sabinene (12.38 %) Myristicine (10.88 %), elemicin (8.93 %), isocoumarin (6.26 %), myristicacid (5.96 %), and "-pinene (4.73 %). ABSTRAK Penelitian ini bertujuan untuk membandingkan komponen penyusun oleoresin biji pala (Myristica fragrans Houtt)yang dibuat dengan cara maserasi langsung dan gabungan distilasi – maserasi. Yield oleoresin pala sebesar 15,17±0,07(% bk) yang diperoleh dengan cara maserasi langsung dan oleoresin hasil ekstraksi gabungan metode distilasi danmaserasi diperoleh yield sebesar 20,07±0,23 (% bk). Sedangkan yield minyak atsiri sendiri dari hasil distilasi air-uapdiperoleh sebesar 6,61 (% bk). Senyawa penyusun oleoresin ekstrak etanol hasil analisis menggunakan metode GCMSteridentiÞ kasi senyawa sebanyak 39 macam dengan komponen yang berada dalam jumlah besar adalah methyleugenol(33,40 %), Myristicine (10,90 %), cis-methyl isoeugenol (9,09 %), elemicin (8,33 %), dan isocoumarin (5,61 %). Untukminyak atsiri biji pala terdapat 31 komponen senyawa, dimana komponen yang berada dalam jumlah yang besar adalahsabinene (34,97 %), !– phellandrene (9,19 %), methyleugenol (7,55 %), Myristicine (5,29 %) dan elimicine (3,21%).Sedangkan untuk minyak atsiri yang dicampur dengan oleoresin dari ampas sisa distilasi terdapat 58 komponen senyawayang menyusun oleoresin campuran tersebut dengan senyawa yang berada dalam jumlah besar yaitu; sabinene (12,38%) Myristicine (10,88 %), elemicin (8,93 %), isocoumarin (6,26 %), myristic acid (5,96 %), dan !- pinene (4,73 %).
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PERBANDINGAN EKSTRAKSI OLEORESIN BIJI PALA (MYRICTICA FRAGRANS HOUTT) ASAL MALUKU UTARA MENGGUNAKAN METODE MASERASI DAN GABUNGAN DISTILASI – MASERASI
Universitas Gadjah Mada, 2013Co-Authors: Muhammad Assagaf, Chusnul Hidayat, Pudji Hastuti, Supriyadi SupriyadiAbstract:PERBANDINGAN EKSTRAKSI OLEORESIN BIJI PALA (MYRICTICA FRAGRANSHOUTT) ASAL MALUKU UTARA MENGGUNAKAN METODE MASERASI DANGABUNGAN DISTILASI – MASERASI Comparison of Nutmeg (Myristica fragrans Houtt) Oleoresin Extraction from North Maluku UsingMaceration and Combination of Distillation-Maceration Methods Muhammad Assagaf1, Pudji Hastuti2, Chusnul Hidayat2, Supriyadi2 1 Balai Pengkajian Teknologi Pertanian (BPTP) Maluku Utara, Jl. Kusu, SoÞ Þ , Kota Tidore Kepulauan 2 Fakultas Teknologi Pertanian Universitas Gadjah Mada, Jl. Flora No. 1, Bulaksumur, Yogyakarta 55281 Email: assagaf_met@yahoo.com ABSTRAK Penelitian ini bertujuan untuk membandingkan komponen penyusun oleoresin biji pala (Myristica fragrans Houtt)yang dibuat dengan cara maserasi langsung dan gabungan distilasi – maserasi. Yield oleoresin pala sebesar 15,17±0,07(% bk) yang diperoleh dengan cara maserasi langsung dan oleoresin hasil ekstraksi gabungan metode distilasi danmaserasi diperoleh yield sebesar 20,07±0,23 (% bk). Sedangkan yield minyak atsiri sendiri dari hasil distilasi air-uapdiperoleh sebesar 6,61 (% bk). Senyawa penyusun oleoresin ekstrak etanol hasil analisis menggunakan metode GCMSteridentiÞ kasi senyawa sebanyak 39 macam dengan komponen yang berada dalam jumlah besar adalah methyleugenol(33,40 %), Myristicine (10,90 %), cis-methyl isoeugenol (9,09 %), elemicin (8,33 %), dan isocoumarin (5,61 %). Untukminyak atsiri biji pala terdapat 31 komponen senyawa, dimana komponen yang berada dalam jumlah yang besar adalahsabinene (34,97 %), !– phellandrene (9,19 %), methyleugenol (7,55 %), Myristicine (5,29 %) dan elimicine (3,21%).Sedangkan untuk minyak atsiri yang dicampur dengan oleoresin dari ampas sisa distilasi terdapat 58 komponen senyawayang menyusun oleoresin campuran tersebut dengan senyawa yang berada dalam jumlah besar yaitu; sabinene (12,38%) Myristicine (10,88 %), elemicin (8,93 %), isocoumarin (6,26 %), myristic acid (5,96 %), dan !- pinene (4,73 %).Kata kunci: minyak atsiri, oleoresin, maserasi, distilasi-maserasi, GC-MS ABSTRACT The purpose of this study was to compare the composition of oleoresin nutmeg (Myristica fragrans Houtt) madedirectly by maceration and combined distillation – maceration. Nutmeg oleoresin yield amounted to 15.17±0.07 (% db)obtained by direct maceration and oleoresin extraction method combined distillation and maceration obtained yield of20.07±0.23 (% db). While the essential oil yield itself from the water-steam distillation of the results obtained at 6.61(% db). Ethanol extract of oleoresin analysis using GCMS method identiÞ ed a total of 39 kinds of compounds withthe composition of major components is methyleugenol (33.40 %), Myristicine (10.90 %), cis-methyl isoeugenol (9.09%), elemicin (8.33 %), and isocoumarin (5.61 %). For nutmeg essential oil contained 31 components of the compound,where the components are located in large numbers was sabinene (34.97 %), !-phellandrene (19.9 %), methyleugenol(7.55 %), Myristicine (5.29 %) and elimicine (3.21 %). As for the essential oil is mixed with the oleoresin from the pulpremaining distillation contained 58 components that make up the compound of the oleoresin with a mixture of maincomponents, namely: sabinene (12.38 %) Myristicine (10.88 %), elemicin (8.93 %), isocoumarin (6.26 %), myristicacid (5.96 %), and "-pinene (4.73 %).Key words: essential oil, oleoresin, maceration, maceration-distillation, GC-M
Fariba Heshmati Afshar - One of the best experts on this subject based on the ideXlab platform.
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comparative toxicity of helosciadium nodiflorum essential oils and combinations of their main constituents against the cabbage looper trichoplusia ni lepidoptera
Industrial Crops and Products, 2017Co-Authors: Kevin Cianfaglione, Filippo Maggi, Fariba Heshmati Afshar, Romilde Iannarelli, Murray B IsmanAbstract:Abstract The chemical composition of the essential oils from the aerial parts of Helosciadium nodiflorum Apiaceae), obtained from two different localities in Italy, were analyzed by gas chromatography/mass spectrometry (GC/MS). Sample 1 (collected from Sulmona) was dominated by phenylpropanoids (49.1%) with Myristicin (49.1%), ( Z )-β-ocimene (19.0%), limonene (7.8%) and terpinolene (7.1%) as major constituents. Sample 2 (collected from Colfiorito) was mainly composed of monoterpene hydrocarbons (58.7%) and the main compounds of the oil were limonene (40.6%), Myristicin (24.3%), dillapiol (9.4%) and β-pinene (5.5%). In order to determine relationships between the chemical composition and insecticidal activity of the oils, comparative and synergistic interactions of the main constituents of H. nodiflorum essential oils were investigated in third-instar larvae of the cabbage looper, Trichoplusia ni , via a contact toxicity bioassay. In the case of sample 1, Myristicin was identified as a major active principle while in sample 2, limonene, Myristicin and dillapiol were main insecticidal constituents. Several combinations of these compounds were synergistic when topically applied, especially Myristicin and ( Z )-β-ocimene, or limonene.
Muhammad Assagaf - One of the best experts on this subject based on the ideXlab platform.
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Perbandingan Ekstraksi Oleoresin Biji Pala (Myrictica Fragrans Houtt) Asal Maluku Utara Menggunakan Metode Maserasi dan Gabungan Distilasi – Maserasi
2013Co-Authors: Muhammad Assagaf, Chusnul Hidayat, Pudji Hastuti, Supriyadi SupriyadiAbstract:The purpose of this study was to compare the composition of oleoresin nutmeg (Myristica fragrans Houtt) madedirectly by maceration and combined distillation – maceration. Nutmeg oleoresin yield amounted to 15.17±0.07 (% db)obtained by direct maceration and oleoresin extraction method combined distillation and maceration obtained yield of20.07±0.23 (% db). While the essential oil yield itself from the water-steam distillation of the results obtained at 6.61(% db). Ethanol extract of oleoresin analysis using GCMS method identiÞ ed a total of 39 kinds of compounds withthe composition of major components is methyleugenol (33.40 %), Myristicine (10.90 %), cis-methyl isoeugenol (9.09%), elemicin (8.33 %), and isocoumarin (5.61 %). For nutmeg essential oil contained 31 components of the compound,where the components are located in large numbers was sabinene (34.97 %), !-phellandrene (19.9 %), methyleugenol(7.55 %), Myristicine (5.29 %) and elimicine (3.21 %). As for the essential oil is mixed with the oleoresin from the pulpremaining distillation contained 58 components that make up the compound of the oleoresin with a mixture of maincomponents, namely: sabinene (12.38 %) Myristicine (10.88 %), elemicin (8.93 %), isocoumarin (6.26 %), myristicacid (5.96 %), and "-pinene (4.73 %). ABSTRAK Penelitian ini bertujuan untuk membandingkan komponen penyusun oleoresin biji pala (Myristica fragrans Houtt)yang dibuat dengan cara maserasi langsung dan gabungan distilasi – maserasi. Yield oleoresin pala sebesar 15,17±0,07(% bk) yang diperoleh dengan cara maserasi langsung dan oleoresin hasil ekstraksi gabungan metode distilasi danmaserasi diperoleh yield sebesar 20,07±0,23 (% bk). Sedangkan yield minyak atsiri sendiri dari hasil distilasi air-uapdiperoleh sebesar 6,61 (% bk). Senyawa penyusun oleoresin ekstrak etanol hasil analisis menggunakan metode GCMSteridentiÞ kasi senyawa sebanyak 39 macam dengan komponen yang berada dalam jumlah besar adalah methyleugenol(33,40 %), Myristicine (10,90 %), cis-methyl isoeugenol (9,09 %), elemicin (8,33 %), dan isocoumarin (5,61 %). Untukminyak atsiri biji pala terdapat 31 komponen senyawa, dimana komponen yang berada dalam jumlah yang besar adalahsabinene (34,97 %), !– phellandrene (9,19 %), methyleugenol (7,55 %), Myristicine (5,29 %) dan elimicine (3,21%).Sedangkan untuk minyak atsiri yang dicampur dengan oleoresin dari ampas sisa distilasi terdapat 58 komponen senyawayang menyusun oleoresin campuran tersebut dengan senyawa yang berada dalam jumlah besar yaitu; sabinene (12,38%) Myristicine (10,88 %), elemicin (8,93 %), isocoumarin (6,26 %), myristic acid (5,96 %), dan !- pinene (4,73 %).
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PERBANDINGAN EKSTRAKSI OLEORESIN BIJI PALA (MYRICTICA FRAGRANS HOUTT) ASAL MALUKU UTARA MENGGUNAKAN METODE MASERASI DAN GABUNGAN DISTILASI – MASERASI
Universitas Gadjah Mada, 2013Co-Authors: Muhammad Assagaf, Chusnul Hidayat, Pudji Hastuti, Supriyadi SupriyadiAbstract:PERBANDINGAN EKSTRAKSI OLEORESIN BIJI PALA (MYRICTICA FRAGRANSHOUTT) ASAL MALUKU UTARA MENGGUNAKAN METODE MASERASI DANGABUNGAN DISTILASI – MASERASI Comparison of Nutmeg (Myristica fragrans Houtt) Oleoresin Extraction from North Maluku UsingMaceration and Combination of Distillation-Maceration Methods Muhammad Assagaf1, Pudji Hastuti2, Chusnul Hidayat2, Supriyadi2 1 Balai Pengkajian Teknologi Pertanian (BPTP) Maluku Utara, Jl. Kusu, SoÞ Þ , Kota Tidore Kepulauan 2 Fakultas Teknologi Pertanian Universitas Gadjah Mada, Jl. Flora No. 1, Bulaksumur, Yogyakarta 55281 Email: assagaf_met@yahoo.com ABSTRAK Penelitian ini bertujuan untuk membandingkan komponen penyusun oleoresin biji pala (Myristica fragrans Houtt)yang dibuat dengan cara maserasi langsung dan gabungan distilasi – maserasi. Yield oleoresin pala sebesar 15,17±0,07(% bk) yang diperoleh dengan cara maserasi langsung dan oleoresin hasil ekstraksi gabungan metode distilasi danmaserasi diperoleh yield sebesar 20,07±0,23 (% bk). Sedangkan yield minyak atsiri sendiri dari hasil distilasi air-uapdiperoleh sebesar 6,61 (% bk). Senyawa penyusun oleoresin ekstrak etanol hasil analisis menggunakan metode GCMSteridentiÞ kasi senyawa sebanyak 39 macam dengan komponen yang berada dalam jumlah besar adalah methyleugenol(33,40 %), Myristicine (10,90 %), cis-methyl isoeugenol (9,09 %), elemicin (8,33 %), dan isocoumarin (5,61 %). Untukminyak atsiri biji pala terdapat 31 komponen senyawa, dimana komponen yang berada dalam jumlah yang besar adalahsabinene (34,97 %), !– phellandrene (9,19 %), methyleugenol (7,55 %), Myristicine (5,29 %) dan elimicine (3,21%).Sedangkan untuk minyak atsiri yang dicampur dengan oleoresin dari ampas sisa distilasi terdapat 58 komponen senyawayang menyusun oleoresin campuran tersebut dengan senyawa yang berada dalam jumlah besar yaitu; sabinene (12,38%) Myristicine (10,88 %), elemicin (8,93 %), isocoumarin (6,26 %), myristic acid (5,96 %), dan !- pinene (4,73 %).Kata kunci: minyak atsiri, oleoresin, maserasi, distilasi-maserasi, GC-MS ABSTRACT The purpose of this study was to compare the composition of oleoresin nutmeg (Myristica fragrans Houtt) madedirectly by maceration and combined distillation – maceration. Nutmeg oleoresin yield amounted to 15.17±0.07 (% db)obtained by direct maceration and oleoresin extraction method combined distillation and maceration obtained yield of20.07±0.23 (% db). While the essential oil yield itself from the water-steam distillation of the results obtained at 6.61(% db). Ethanol extract of oleoresin analysis using GCMS method identiÞ ed a total of 39 kinds of compounds withthe composition of major components is methyleugenol (33.40 %), Myristicine (10.90 %), cis-methyl isoeugenol (9.09%), elemicin (8.33 %), and isocoumarin (5.61 %). For nutmeg essential oil contained 31 components of the compound,where the components are located in large numbers was sabinene (34.97 %), !-phellandrene (19.9 %), methyleugenol(7.55 %), Myristicine (5.29 %) and elimicine (3.21 %). As for the essential oil is mixed with the oleoresin from the pulpremaining distillation contained 58 components that make up the compound of the oleoresin with a mixture of maincomponents, namely: sabinene (12.38 %) Myristicine (10.88 %), elemicin (8.93 %), isocoumarin (6.26 %), myristicacid (5.96 %), and "-pinene (4.73 %).Key words: essential oil, oleoresin, maceration, maceration-distillation, GC-M
Murray B Isman - One of the best experts on this subject based on the ideXlab platform.
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comparative toxicity of helosciadium nodiflorum essential oils and combinations of their main constituents against the cabbage looper trichoplusia ni lepidoptera
Industrial Crops and Products, 2017Co-Authors: Kevin Cianfaglione, Filippo Maggi, Fariba Heshmati Afshar, Romilde Iannarelli, Murray B IsmanAbstract:Abstract The chemical composition of the essential oils from the aerial parts of Helosciadium nodiflorum Apiaceae), obtained from two different localities in Italy, were analyzed by gas chromatography/mass spectrometry (GC/MS). Sample 1 (collected from Sulmona) was dominated by phenylpropanoids (49.1%) with Myristicin (49.1%), ( Z )-β-ocimene (19.0%), limonene (7.8%) and terpinolene (7.1%) as major constituents. Sample 2 (collected from Colfiorito) was mainly composed of monoterpene hydrocarbons (58.7%) and the main compounds of the oil were limonene (40.6%), Myristicin (24.3%), dillapiol (9.4%) and β-pinene (5.5%). In order to determine relationships between the chemical composition and insecticidal activity of the oils, comparative and synergistic interactions of the main constituents of H. nodiflorum essential oils were investigated in third-instar larvae of the cabbage looper, Trichoplusia ni , via a contact toxicity bioassay. In the case of sample 1, Myristicin was identified as a major active principle while in sample 2, limonene, Myristicin and dillapiol were main insecticidal constituents. Several combinations of these compounds were synergistic when topically applied, especially Myristicin and ( Z )-β-ocimene, or limonene.
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insecticidal activity of the essential oil of ligusticum mutellina roots
Zeitschrift für Naturforschung C, 2005Co-Authors: Claus M Passreiter, Yasmin Akhtar, Murray B IsmanAbstract:The essential oil obtained from roots of different collections of Ligusticum mutellina was tested against 3 r d instar armyworms, Pseudaletia unipuncta (Lepidoptera: Noctuidae), for insecticidal activity. The main compounds were isolated and their structures were elucidated using 2D-NMR techniques. Our collections contained dillapiole, ligustilide and Myristicin as major compounds. The previously reported sarisan was not present, moreover its occurrence in L. mutellina should be revised based on our findings.
Karwur, Ferry F. - One of the best experts on this subject based on the ideXlab platform.
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ISOLASI DAN IDENTIFIKASI KOMPONEN KIMIA MINYAK ASIRI DAGING BUAH DAN FULI BERDASARKAN UMUR BUAH PALA (MYRISTICA FRAGRANS HOUTT)
'Universitas Mataram', 2020Co-Authors: Liunokas, Angreni B., Karwur, Ferry F.Abstract:Abstrak: Pala (Myristica fragrans Houtt) sebagai bioreaktor hayati menghasilkan produk utama minyak asiri bernilai ekonomi tinggi yang tersebar pada bagian-bagian buahnya. Minyak asiri pala tersusun oleh kelompok besar terpenoid dan fenilpropanoid yang memiliki konsentrasi terkecil namun sebagai indikator mutu minyak pala. Penelitian tentang isolasi dan identifikasi komponen kimia minyak asiri daging buah dan fuli pala, telah dilaksanakan di Laboratorium CARC UKSW Salatiga dan Laboratorium Terpadu UII Yogyakarta. Penelitian ini bertujuan untuk mengetahui komponen kimia minyak asiri daging buah dan fuli pala berdasarkan tahapan perkembangan buah dan isolasi miristisin sebagai indikator dari kualitas minyak pala. Minyak asiri diperoleh dengan metode ekstraksi kemudian di analisis komponennya menggunakan Kromatografi Gas Spektrometri Massa (GC-MS). Hasil penelitian menunjukkan bahwa komponen kimia terbesar dari minyak asiri daging buah pala secara berturut-turut yaitu tahap pertama miristisin 36.05% pada retensi 11.57 menit, tahap kedua dan keempat α-pinen 39.16%; 34.64% retensi 3.53 menit, tahap ketiga sabinen 33.88% pada retensi 3.99 menit. Sedangkan pada minyak fuli tahap pertama hingga keempat yaitu sabinen 38.72%; 37.51%; 36.24%; 28.93% pada waktu retensi 3.99. Berdasarkan analisis GC-MS menunjukkan bahwa komponen senyawa yang dominan pada daging buah dan fuli yaitu miristisin, sabinen, α-pinen, β-pinen yang berkontribusi bagi aroma khas pada pala. Hasil penelitian diharapkan dapat dimanfaatkan sebagai sumber informasi penting dalam menghasilkan minyak asiri dengan kualitas baik dengan kandungan miristisin terbanyak.Kata Kunci : M. fragrans Houtt; isolasi; daging buah, fuli, minyak asiriAbstract: Nutmeg (Myristica fragrans Houtt) as a natural bioreactor produces the main product that is aetheric oil with a high economic value which is scattered on the parts of the fruit. Aetheric oil consists of a big group of terpenoid and phenylpropanoid which has the smallest concentration but functions as the indicator of nutmeg oil quality. The research about isolation and identification of chemical components of aetheric oil of pulp and mace has been conducted in CARC Laboratory of UKSW Salatiga and Integrated Laboratory of UII Yogyakarta. This current research aims at knowing the components of aetheric oil of nutmeg pulp and mace based on the development stages of the fruit and Myristicin isolation as the indicator of the quality of nutmeg oil. Aetheric oil is formed by the extraction method. Then the components are analyzed by using Mass Spectrometry Gass Chromatography (GC-MS). The result of the research shows that respectively the biggest chemical component of aetheric oil consists of the first stage Myristicin 36.05% on retention 11.57 minutes, second stage and fourth stage α-pinene 39.16%; 34.64% on retention 3.53 minutes, the third stage sabinene 33.88% on retention 3.99 minutes. Meanwhile on the mace oil, the first to the fourth stage is sabinene 38.72%; 37.51%; 36.24%; 28.93% on retention 3.99. Based on the analysis of GC-MS, it is shown that the most dominant compound components of pulp and mace are Myristicin, sabinene, α-pinene, and β-pinene which contribute to the typical scent of nutmeg. The result of the research is expected to be used as an important information source in resulting in aetheric oil with good quality with the most Myristicin content.Keywords: Myristica fragrans Houtt; isolation; pulp, mace, aetheric oi
